Applied Geoscience Laboratory

The Applied Geoscience Laboratory is the University of Edinburgh's specialist experimental research facility dedicated to understanding the behaviour of subsurface materials and engineered systems under representative in-situ subsurface conditions. Through internationally leading research, strategic collaborations and industrial partnerships, we advance the science underpinning the safe, secure and sustainable use of the subsurface in support of the energy transition.

Our bespoke, purpose-built experimental facilities recreate representative subsurface conditions of temperature, pressure, geochemistry, multiphase fluid flow and coupled thermal, hydraulic, mechanical, chemical and biological (THMCB) processes. Integrated with advanced rock, fluid, gas and microbial characterisation capabilities, they enable end-to-end investigations of subsurface systems from the pore scale through to the reservoir scale. Together they enable both fundamental and applied research across underground hydrogen storage, carbon capture and geological storage (CCS), geothermal energy, compressed air energy storage (CAES), underground gas storage, natural hydrogen, well integrity, geological disposal of radioactive waste and wider subsurface energy and environmental systems.

Established in 2009, the Applied Geoscience Laboratory has grown into one of the UK's leading experimental research facilities for subsurface energy systems. Today, the laboratory supports major UK and international research programmes, strategic industrial partnerships and collaborative projects across the energy and environmental sectors. Our multidisciplinary expertise spans geochemistry, geomicrobiology, petrophysics, geomechanics, well integrity, reactive transport and pore-scale imaging, underpinning projects that range from discovery science and technology development through to industrial innovation and regulatory evidence generation.The laboratory forms part of the European research infrastructure ECCSEL (European Carbon Dioxide Capture and Storage Laboratory Infrastructure), supporting international collaboration and providing access to world-class experimental research infrastructure for subsurface energy and environmental systems.

Alongside our internationally funded research programmes, we work closely with industry, government and research organisations to deliver collaborative research, specialist laboratory testing, independent technical consultancy and collaborative research. By integrating world-leading research with practical application, we help address both fundamental scientific questions and industry-led technical challenges.

Contact and location

Contact

Professor Katriona Edlmann kedlmann@ed.ac.uk+44 (0) 131 650 7238Chair in Sustainable Energy

View Professor Edlmann's full research profile

Location

Address: Room 236, Grant Institute, School of GeoSciences, University of Edinburgh, West Mains Road, EDINBURGH EH9 3JW

Please note that parking on campus is strictly by permit only, and parking spaces are subject to availability. Commercial and external users should contact our staff about parking arrangements.

We welcome enquiries at all stages of project development whether you are seeking access to our experimental facilities, exploring opportunities for collaborative research, developing a new project or requiring specialist laboratory testing or technical consultancy. 

Our multidisciplinary team is happy to discuss experimental design, technical feasibility and potential research partnerships.

We welcome enquiries from researchers, industrial partners, government agencies, regulators and funding organisations interested in advancing the safe, secure and sustainable use of the subsurface.

Facilities and equipment

Each facility can be configured as part of bespoke experimental programmes tailored to specific scientific, engineering and operational challenges, enabling collaborative research, technology development and independent laboratory testing.

Reservoir flow and transport

•    High Pressure THMC Multiphase Flow System (formerly THMC Multiphase Flow Rig)
•    Long-Core Gas Transport System (formerly Hydrogen Flow Rig)
•    Low Pressure Soil Column Flow System (new) 

High pressure geochemistry and geobiology

•    High Pressure Geochemical Reaction System (formerly Hydrogen Reaction Vessels)
•    High Temperature Batch Reaction System (Parr vessels)
•    Low Pressure Batch Reaction System (new) 

Rock mechanics and reservoir integrity

•    Large Scale Geomechanical Testing System (formerly Unconfined Loading Rig)
•    Thermal Cycling and Freeze-Thaw System (formerly Freeze Thaw Rig) 

Pore scale imaging and visualisation

•    Multiphase Microfluidic Flow System
•    X-ray Transparent Micro-CT Flow System (formerly Micro-CT Hydrogen Flow Cell)
 

The High Pressure THMC Multiphase Flow System is a bespoke core flooding facility designed to investigate coupled thermal, hydraulic, mechanical, chemical and biological (THMCB) processes under representative subsurface pressure, temperature and geochemical conditions. The system enables controlled single and multiphase flow through reservoir core samples while independently controlling confining stress, pore pressure, effective stress, temperature, fluid composition and flow rate. Integrated fluid sampling and continuous monitoring allow the investigation of reactive transport processes, reservoir behaviour and fluid-rock interactions during dynamic flow experiments.

Key capabilities

ParameterCapability
Confining pressureUp to 60 MPa radial confining stress (σ₂ = σ₃)
Pore fluid pressureUp to 60 MPa
Rock temperatureUp to 80°C
Injection fluid temperatureUp to 80°C
Sample size38 mm diameter cores up to 80 mm length
Flow regimeSingle and multiphase flow
Compatible fluidsHydrogen, carbon dioxide (gas, liquid and supercritical), methane, nitrogen, oxygen, air, water, representative formation brines and tracers
Flow rate0.001–20 ml/min (pump dependent)
PumpsISCO syringe pumps, CP Class positive displacement pumps, Cetoni dual syringe pumps
MonitoringUpstream, downstream and differential pressure measurement
SamplingContinuous fluid sampling during experiments
Materials316 stainless steel and PEEK wetted components for corrosion resistance
ControlFully computer-controlled operation and data logging

Example Research applications

  • Relative permeability and capillary pressure
  • Multiphase flow behaviour
  • Reactive transport
  • Water-rock interaction
  • Hydrogen-rock interaction
  • CO₂-rock interaction
  • Gas-brine interaction
  • Reservoir injectivity and productivity
  • Formation damage
  • Permeability evolution
  • Wettability alteration
  • Residual trapping
  • Cushion gas optimisation
  • Cyclic gas storage
  • Contaminant transport
  • Enhanced geothermal systems
  • Reservoir analogue studies
  • Validation of numerical reservoir models

The Long-Core Gas Transport System is a bespoke experimental facility designed to quantify gas transport through porous geological materials under controlled pressure and temperature conditions. Unlike conventional laboratory core flooding systems, the facility accommodates 1 m long rock cores, providing a more representative experimental scale for investigating gas transport through heterogeneous geological formations. Coupled with a Hiden HPR-20 mass spectrometer, the system enables high-resolution, real-time gas composition and breakthrough analysis to investigate gas migration, mixing and transport processes through porous media. The facility enables direct measurement of the fundamental transport parameters—including advective velocity, mechanical dispersion, molecular diffusion and gas sorption—that underpin predictive models of subsurface gas flow. It supports research across underground hydrogen and natural gas storage, carbon capture and geological storage (CCS), geothermal energy, environmental monitoring and reservoir characterisation.

ParameterCapability
Core size1 m long × 38 mm diameter sandstone core
Gas pressureUp to 1 MPa
Rock temperatureUp to 60°C
Injection gas temperatureUp to 60°C
Compatible gasesHydrogen, carbon dioxide, methane, oxygen, nitrogen, air, noble gases, SF₆ and other tracer gases
Flow regimeSingle and multiphase gas flow
Flow rate0.01–10 ml/min
MonitoringUpstream, downstream and differential pressure measurement
Gas analysisHiden HPR-20 mass spectrometer
ConstructionGas-tight foil, resin and stainless-steel core assembly
ControlContinuous monitoring and computerised data acquisition

Example research applications

  • Gas breakthrough analysis
  • Advective transport
  • Mechanical dispersion
  • Molecular diffusion
  • Gas sorption and retardation
  • Tracer gas experiments
  • Reservoir characterisation
  • Gas migration studies
  • Hydrogen transport
  • Carbon dioxide transport
  • Methane transport
  • Gas mixing behaviour
  • Formation heterogeneity assessment
  • Effective porosity determination
  • Transport parameter determination for reservoir simulation
  • Validation of reactive transport and reservoir models
  • Monitoring technology development
  • Gas quality and contaminant transport studies

The Low Pressure Soil Column Flow System is a bespoke experimental facility designed to investigate gas transport, reactive processes and biogeochemical interactions within soils and unconsolidated sediments under controlled laboratory conditions. The instrumented soil columns enable investigation of gas migration, leakage behaviour, soil–gas interactions and microbial processes across a wide range of environmental conditions. Continuous monitoring of gas composition, pH, redox potential, temperature and moisture provides detailed characterisation of coupled physical, chemical and biological processes during gas transport experiments. The facility supports research into environmental impacts, leak detection, near-surface monitoring and reactive transport associated with energy infrastructure and wider environmental systems.

ParameterCapability
Experimental scaleInstrumented one-dimensional soil columns
PressureAtmospheric to low pressure gas flow
TemperatureAmbient and controlled temperature conditions
Compatible gasesHydrogen, carbon dioxide, methane, oxygen, nitrogen, air, noble gases and tracer gases
MaterialsNatural soils, engineered soils, unconsolidated sediments, sand packs and synthetic porous media
Experimental conditionsVariable moisture content, porosity, layering and gas injection rates
Gas monitoringContinuous gas sampling and gas composition analysis
Water chemistryPeriodic pore-water sampling
Geochemical monitoringContinuous pH and redox (Eh) measurements
SpectrophotometryUV-Visible spectrophotometric analysis (520 nm and other wavelengths)
Environmental controlMoisture, temperature and gas composition control
SamplingGas, pore-water and solid sampling throughout experiments

Typical research applications

  • Gas migration through soils
  • Hydrogen leakage from buried infrastructure
  • Methane migration
  • Carbon dioxide leakage studies
  • Tracer gas investigations
  • Soil-gas interactions
  • Reactive transport
  • Soil geochemistry
  • Soil microbiology
  • Soil redox evolution
  • Soil carbon cycling
  • Environmental monitoring
  • Leak detection technology development
  • Soil remediation studies
  • Contaminant transport
  • Vadose zone processes
  • Groundwater recharge investigations
  • Natural hydrogen investigations
  • Validation of environmental transport models

The High Pressure Geochemical and Geobiological Reaction Systems comprise a comprehensive suite of more than twelve bespoke batch reaction vessels designed to investigate fluid-rock-gas-microbe interactions under representative subsurface conditions. The facility accommodates a wide range of experimental pressures, temperatures and vessel volumes, providing exceptional flexibility for investigating geological materials, engineered systems and microbial processes across subsurface energy and environmental applications.

The independently operated reaction vessels incorporate controlled heating, magnetic stirring, pressure monitoring and custom sampling systems, allowing liquid and gas samples to be collected throughout an experiment without disturbing reaction conditions. The facility supports both sterile and biologically active experimental programmes through dedicated UV and autoclave sterilisation capabilities, enabling robust comparison of abiotic and microbially mediated processes. Multiple reaction vessels can be operated simultaneously, allowing statistically robust experimental programmes incorporating controls, replicate testing and time-series investigations.

The availability of multiple independently operated reaction vessels with different pressure, temperature and volume capabilities enables bespoke experimental programmes to be designed around specific scientific, engineering and operational questions rather than the constraints of a single reactor configuration.

ParameterCapability
Reaction systemsMore than 12 independently operated high-pressure batch reaction vessels
Vessel volumesMultiple vessel sizes (including 300 ml and larger/smaller configurations)
PressureAtmospheric to 200 bar (20 MPa)*
TemperatureAmbient to 300°C*
HeatingIndependently controlled heating systems
MixingMagnetic stirring and agitation
Compatible gasesHydrogen, carbon dioxide, methane, oxygen, nitrogen, air, noble gases and bespoke gas mixtures
Compatible fluidsFreshwater, formation brines, geothermal fluids, produced waters and bespoke experimental solutions
Sample materialsRocks, minerals, sediments, soils, well cements, steels, engineered materials and microbial cultures
SamplingTime-series liquid and gas sampling via dip tubes without interrupting experiments
MonitoringContinuous pressure and temperature monitoring
Experimental conditionsSterile or biologically active (non-sterile) experimental programmes
SterilisationUV and autoclave sterilisation for contamination control and experimental preparation
Experimental durationHours to many months

Example research applications

  • Water-rock interaction
  • Water-gas-rock interaction
  • Hydrogen-rock interaction
  • Carbon dioxide-rock interaction
  • Methane-rock interaction
  • Oxygen reactivity studies
  • Mineral dissolution and precipitation
  • Gas quality evolution
  • Formation water evolution
  • Corrosion and materials compatibility
  • Well cement integrity
  • Steel degradation
  • Geomicrobiology
  • Biogeochemistry
  • Microbially mediated gas generation and consumption
  • Redox evolution
  • Sulphide generation
  • Carbon mineralisation
  • Critical mineral recovery
  • Geothermal fluid chemistry
  • Geological disposal of radioactive waste
  • Environmental geochemistry
  • Long-term ageing experiments
  • Accelerated reaction studies

The Low Pressure Batch Reaction Systems comprise a suite of four jacketed glass reactor systems designed for controlled geochemical, geomicrobiological and environmental reaction experiments under ambient and low-pressure conditions. The systems provide precise control of temperature, mixing and fluid chemistry, making them ideally suited to rapid experimental screening, kinetic studies and long-duration reaction experiments where representative reservoir pressures are not required.

Each reactor incorporates continuous stirring, temperature control and multiple access ports for fluid and gas sampling, allowing reaction progress to be monitored throughout an experiment without disturbing the system. Their flexible configuration makes them particularly valuable for high-throughput experimental screening, method development and comparative studies. The transparent reaction vessels facilitate direct observation of reaction pathways, complementing quantitative geochemical and microbiological analyses.

The low-pressure systems complement the laboratory’s high-pressure reaction facilities by providing a flexible platform for rapid experimental screening, method development and mechanistic studies prior to high-pressure experimentation.

ParameterCapability
Reaction systemsFour independently operated jacketed glass batch reactors
Vessel volume300 ml
PressureAtmospheric to low-pressure operation
TemperatureControlled heated or cooled reaction conditions via external circulating bath
HeatingDouble-jacketed temperature-controlled vessels
MixingVariable-speed mechanical stirring
Compatible gasesHydrogen, carbon dioxide, methane, oxygen, nitrogen, air and bespoke gas mixtures
Compatible fluidsFreshwater, groundwater, formation brines and bespoke experimental solutions
Sample materialsRocks, minerals, soils, sediments, well cements, engineered materials and microbial cultures
SamplingRepeated liquid and gas sampling throughout experiments
MonitoringContinuous temperature monitoring with optional pH and redox (Eh) measurement
Experimental conditionsSterile or biologically active (non-sterile) experimental programmes
SterilisationUV and autoclave sterilisation for contamination control and experimental preparation
Visual accessTransparent glass vessels enable direct observation of reaction processes
Experimental durationHours to many months

Example research applications

  • Geochemical reaction kinetics
  • Water-rock interaction
  • Water-gas-rock interaction
  • Soil-water interaction
  • Gas dissolution studies
  • Mineral dissolution and precipitation
  • Geomicrobiology
  • Biogeochemistry
  • Microbial growth and activity
  • Environmental geochemistry
  • Batch adsorption and desorption experiments
  • Contaminant degradation
  • Nutrient cycling
  • Method development
  • Experimental screening
  • Comparative testing
  • Long-duration environmental experiments
  • Teaching and demonstration experiments

The Large Scale Geomechanical Testing System is a bespoke experimental facility designed to investigate the mechanical behaviour, deformation and long-term integrity of large geological specimens under controlled unconfined loading conditions. Accommodating rock samples up to 200 mm in diameter, the system enables investigation of deformation, creep and hydraulic fracturing at a scale more representative of subsurface rock masses than conventional laboratory core testing. The facility supports research into reservoir geomechanics, rock mechanics and well integrity across a wide range of subsurface energy and environmental applications.

The system provides independent control of axial loading, pore fluid pressure and temperature, together with continuous monitoring of displacement, pore pressure, gas composition and acoustic activity. High-resolution LVDTs provide continuous measurement of sample deformation, while an Itasca Acoustic Emission System and integrated P-wave and S-wave velocity sensors enable the initiation and evolution of micro-fracturing, fracture propagation and changes in elastic properties to be monitored throughout an experiment. The facility is particularly well suited to long-duration creep testing, deformation studies and controlled hydraulic fracturing experiments.

ParameterCapability
Sample sizeUp to 200 mm diameter × 200 mm length
Loading configurationUnconfined axial loading
Mechanical loadingUp to 700 bar applied load
Pore pressureUp to 70 MPa
Rock temperatureUp to 60°C
Injection fluid temperatureUp to 60°C
Compatible fluidsWater and formation brines
Compatible gasesHydrogen, carbon dioxide, methane, oxygen, nitrogen, air and bespoke gas mixtures
Displacement monitoringHigh-resolution LVDTs
Pore pressure monitoringContinuous measurement and data logging
Acoustic monitoringItasca Acoustic Emission System
Ultrasonic monitoringIntegrated P-wave and S-wave velocity sensors
Gas analysisHiden HPR-20 mass spectrometer
Experimental capabilityLong-duration creep, deformation and hydraulic fracturing experiments
Experimental durationShort-term loading through to long-duration testing

Example research applications

  • Rock deformation
  • Time-dependent creep
  • Salt creep
  • Reservoir geomechanics
  • Reservoir integrity
  • Well integrity
  • Underground hydrogen storage
  • Carbon capture and geological storage (CCS)
  • Underground gas storage
  • Geothermal reservoirs
  • Geological disposal of radioactive waste
  • Hydraulic fracturing
  • Fracture initiation and propagation
  • Breakdown pressure determination
  • Injectivity studies
  • Coupled hydro-mechanical behaviour
  • Acoustic emission monitoring
  • P-wave and S-wave velocity evolution
  • Rock damage characterisation
  • Constitutive model development and validation

The Thermal Cycling and Freeze-Thaw System is a bespoke experimental facility designed to investigate the thermo-mechanical behaviour of geological materials subjected to repeated heating, cooling and rapid temperature changes. The facility enables controlled thermal cycling and Joule-Thomson cooling experiments to investigate deformation, fracture development and material integrity under representative subsurface conditions.

The system accommodates both laboratory-scale and large-format rock specimens and incorporates integrated thermal, mechanical and geophysical monitoring throughout each experiment. High-resolution fibre optic strain sensing, temperature monitoring, X-ray computed tomography (CT) and three-dimensional fracture surface analysis provide comprehensive characterisation of damage evolution and rock response during thermal cycling. The facility is particularly well suited to investigating freeze-thaw processes, thermal fatigue and coupled thermo-mechanical behaviour associated with subsurface energy and environmental systems.

ParameterCapability
Sample size38 mm and 200 mm diameter rock and transparent analogue samples
HeatingControlled heating up to 80°C
CoolingJoule-Thomson cooling to -55°C through controlled CO₂ depressurisation
Thermal cyclingRepeated heating and cooling cycles
Strain monitoringHigh-resolution distributed fibre optic strain measurements (LUNA ODiSI-B)
Temperature monitoringContinuous thermal monitoring throughout experiments
Gas analysisHiden HPR-20 mass spectrometer
ImagingX-ray Computed Tomography (CT)
Surface characterisationHigh-resolution 3D fracture surface scanning (GOM ATOS III)
Experimental capabilityLong-duration thermal cycling and freeze-thaw testing

Example research applications

  • Freeze-thaw behaviour
  • Joule-Thomson cooling
  • Thermal cycling
  • Thermal fatigue
  • Rock deformation
  • Fracture initiation and propagation
  • Thermally induced damage
  • Reservoir integrity
  • Well integrity
  • Underground hydrogen storage
  • Carbon capture and geological storage (CCS)
  • Underground gas storage
  • Geothermal systems
  • Thermal energy storage
  • Mechanical property evolution
  • Crack growth monitoring
  • Fibre optic sensing validation
  • Numerical model validation

The Multiphase Microfluidic Flow System is a bespoke experimental facility designed to visualise and quantify single and multiphase fluid flow processes at the pore scale under controlled pressure and temperature conditions. Using optically transparent microfluidic flow cells that replicate representative pore network geometries, the system enables direct observation of fluid displacement, gas migration, fluid-rock interactions and microbial processes that cannot be observed within conventional rock core experiments.

The facility combines high-resolution optical imaging with precise control of pressure, flow rate, fluid composition and temperature, enabling real-time investigation of coupled thermal, hydraulic, chemical and biological (THCB) processes at the pore scale. A wide range of interchangeable micromodel geometries and surface wettabilities allows systematic investigation of the influence of pore structure, wettability, fluid properties and microbial activity on multiphase flow behaviour. The system is particularly well suited to investigating pore-scale transport, reactive processes, biofilm development and validation of pore-network and reservoir simulation models.

ParameterCapability
PressureUp to 100 bar (10 MPa)
TemperatureAmbient to 80°C
Flow regimeSingle and multiphase flow
Compatible fluidsWater, formation brines and bespoke experimental solutions
Compatible gasesHydrogen, carbon dioxide, methane, oxygen, nitrogen, air and bespoke gas mixtures
Flow controlISCO, Cetoni and InfusionONE syringe pumps
Flow rate0.001–20 ml/min (pump dependent)
MicromodelsGlass microfluidic flow cells with variable pore geometries and wettability characteristics
ImagingHigh-resolution optical imaging and video capture
IlluminationWhite light and UV illumination
MonitoringUpstream, downstream and differential pressure measurement
Flow capabilitySteady-state and pulsed flow experiments
Biological capabilitySterile and biologically active flow experiments, including microbial transport and biofilm growth
SamplingEffluent fluid sampling
ControlFully computer-controlled operation and data logging

Example research applications

  • Single and multiphase flow
  • Pore-scale displacement processes
  • Hydrogen migration
  • Carbon dioxide migration
  • Methane migration
  • Gas mixing
  • Residual and capillary trapping
  • Wettability alteration
  • Fluid-fluid interactions
  • Fluid-rock interactions
  • Haines jumps and pore-filling mechanisms
  • Bubble mobilisation
  • Fingering phenomena
  • Reactive transport
  • Contaminant transport
  • Microbial transport
  • Biofilm growth and development
  • Microbial attachment and detachment
  • Microbe-fluid-rock interactions
  • Biogeochemical processes
  • Surface chemistry
  • Validation of pore-network models
  • Reservoir simulation validation

The X-ray Transparent Micro-CT Flow System is a bespoke experimental facility developed by the Applied Geoscience Laboratory to enable real-time visualisation of multiphase fluid flow within natural rock samples under representative subsurface conditions. Originally designed for pore-scale investigations of underground hydrogen storage, the system combines controlled fluid injection with high-resolution X-ray computed tomography (micro-CT) to quantify dynamic flow processes that cannot be observed using conventional laboratory techniques.

The heart of the system is a bespoke carbon fibre-reinforced PEEK pressure vessel that is fully compatible with laboratory micro-CT scanners and national synchrotron facilities, including the Diamond Light Source, where it has been successfully deployed to perform time-resolved (4D) imaging of hydrogen displacement, trapping and connectivity within porous sandstones. These experiments provided the first direct observations of hydrogen displacement mechanisms, Haines jumps and intermittent pore-scale flow during geological hydrogen storage.

The facility enables continuous imaging during fluid injection without interrupting flow, allowing dynamic displacement processes, residual trapping, pore connectivity and fluid distribution to be quantified in three dimensions. Combined with advanced image analysis, the system provides unique insight into the physical processes governing multiphase flow within porous geological materials.

ParameterCapability
Sample sizeApproximately 5 mm diameter × up to 60 mm length rock cores
Confining pressureUp to 10 MPa
Pore pressureUp to 10 MPa
TemperatureAmbient to 80°C
Flow regimeSingle and multiphase flow
Compatible fluidsWater, formation brines and bespoke experimental solutions
Compatible gasesHydrogen, carbon dioxide, methane, oxygen, nitrogen, air and bespoke gas mixtures
Flow controlISCO, Cetoni and InfusionONE syringe pumps
Flow rate0.001–20 ml/min (pump dependent)
Pressure monitoringUpstream, downstream and differential pressure measurement
SamplingEffluent fluid sampling
ImagingLaboratory X-ray micro-CT and synchrotron X-ray CT compatible
Image analysis3D and 4D image reconstruction, segmentation and quantitative pore-scale analysis
ControlFully computer-controlled operation and data logging

Example research applications

  • Underground hydrogen storage 
  • Carbon capture and geological storage (CCS) 
  • Underground gas storage 
  • Geothermal systems 
  • Pore-scale multiphase flow 
  • Hydrogen displacement and recovery 
  • Carbon dioxide displacement 
  • Methane displacement 
  • Residual and capillary trapping 
  • Relative permeability studies 
  • Wettability characterisation 
  • Pore-scale connectivity 
  • Haines jumps 
  • Intermittent flow behaviour 
  • Bubble mobilisation 
  • Fluid distribution and phase evolution 
  • Reactive transport 
  • Reservoir simulation validation 
  • Digital rock physics 
  • Image-based numerical modelling

You can also read Professor Edlmann's blog for further information about the Applied Geoscience Laboratory